Electron backscatter diffraction in materials characterization
نویسندگان
چکیده
Electron Back-Scatter Diffraction (EBSD) is a powerful technique that captures electron diffraction patterns from crystals, constituents of material. Captured patterns can then be used to determine grain morphology, crystallographic orientation and chemistry of present phases, which provide complete characterization of microstructure and strong correlation to both properties and performance of materials. Key milestones related to technological developments of EBSD technique have been outlined along with possible applications using modern EBSD system. Principles of crystal diffraction with description of crystallographic orientation, orientation determination and phase identification have been described. Image quality, resolution and speed, and system calibration have also been discussed. Sample preparation methods were reviewed and EBSD application in conjunction with other characterization techniques on a variety of materials has been presented for several case studies. In summary, an outlook for EBSD technique was provided.
منابع مشابه
EBSD characterization of nano/ultrafine structured Al/Brass composite produced by severe plastic deformation
In the present work, nano/ultrafine structured Al/Brass composite was produced by accumulative roll bonding (ARB) up to eight cycles. The evolution of grain refinement and deformation texture and their effect on the mechanical properties were investigated. It was observed that by increasing the ARB cycles, due to the difference in flow properties of the metal constituents, brass layers necked, ...
متن کاملCrystallographic preferred orientations analysis of quartz crystals in Psammite using electron backscatter diffraction,western Ireland
The present study investigates the crystal preferred orientation (CPO) of quartz crystals in psammitic rocks to ascertain the deformationmechanism using electron backscatter diffraction (EBSD) on quartz crystals from north of the Renvyle-Bofin Slide (RBS) nearLetterfrack in western Ireland. Complete crystallographic orientations were determined for several thousand individual quartz crystalsin ...
متن کاملValidation of three-dimensional diffraction contrast tomography reconstructions by means of electron backscatter diffraction characterization
Microstructure reconstructions resulting from diffraction contrast tomography data of polycrystalline bulk strontium titanate were reinvestigated by means of electron backscatter diffraction (EBSD) characterization. Corresponding two-dimensional grain maps from the two characterization methods were aligned and compared, focusing on the spatial resolution at the internal interfaces. The compared...
متن کاملElectron Backscatter Diffraction (EBSD) Technique and Materials Characterization Examples
The term “electron backscatter diffraction” (EBSD) is now synonymous with both the scanning electron microscope (SEM) technique and the accessory system that can be attached to an SEM. EBSD provides quantitative microstructural information about the crystallographic nature of metals, minerals, semiconductors, and ceramics—in fact most inorganic crystalline materials. It reveals grain size, grai...
متن کاملThree-Dimensional Characterization of Microstructure by Electron Back-Scatter Diffraction
The characterization of microstructures in three dimensions is reviewed, with an emphasis on the use of automated electron backscatter diffraction techniques. Both statistical reconstruction of polycrystalline structures from multiple cross sections and reconstruction from parallel, serial sections are discussed. In addition, statistical reconstruction of second-phase particle microstructures f...
متن کامل